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Various planar technologies are employed for developing solid-state sensors having low cost, small size and high reproducibility; thin- and thick-film technologies are most suitable for such productions. Screen-printing is especially suitable due to its simplicity, low-cost, high reproducibility and efficiency in large-scale production. This technology enables the deposition of a thick layer and allows precise pattern control. Moreover, this is a highly economic technology, saving large amounts of the used inks. In the course of repetitions of the film-deposition procedure there is no waste of material due to additivity of this thick-film technology. Finally, the thick films can be easily and quickly deposited on inexpensive substrates. In this contribution, thick-film ion-selective electrodes based on ionophores as well as crystalline ion-selective materials dedicated for potentiometric measurements are demonstrated. Analytical parameters of these sensors are comparable with those reported for conventional potentiometric electrodes. All mentioned thick-film strip electrodes have been totally fabricated in only one, fully automated thickfilm technology, without any additional manual, chemical or electrochemical steps. In all cases simple, inexpensive, commercially available materials, i.e. flexible, plastic substrates and easily cured polymer-based pastes were used.
Micromachined thermal heater platforms offer low electrical power consumption and high modulation speed, i.e. properties which are advantageous for realizing nondispersive infrared (NDIR) gas- and liquid monitoring systems. In this paper, we report on investigations on silicon-on-insulator (SOI) based infrared (IR) emitter devices heated by employing different kinds of metallic and semiconductor heater materials. Our results clearly reveal the superior high-temperature performance of semiconductor over metallic heater materials. Long-term stable emitter operation in the vicinity of 1300 K could be attained using heavily antimony-doped tin dioxide (SnO2:Sb) heater elements.
Hydrophobic magnetic nanoparticles (NPs) consisting of undecanoate-capped magnetite (Fe3O4, average diameter ca. 5 nm) are used to control quantized electron transfer to surface-confined redox units and metal NPs. A two-phase system consisting of an aqueous electrolyte solution and a toluene phase that includes the suspended undecanoatecapped magnetic NPs is used to control the interfacial properties of the electrode surface. The attracted magnetic NPs form a hydrophobic layer on the electrode surface resulting in the change of the mechanisms of the surface-confined electrochemical processes. A quinone-monolayer modified Au electrode demonstrates an aqueous-type of the electrochemical process (2e-+2H+ redox mechanism) for the quinone units in the absence of the hydrophobic magnetic NPs, while the attraction of the magnetic NPs to the surface results in the stepwise single-electron transfer mechanism characteristic of a dry nonaqueous medium. Also, the attraction of the hydrophobic magnetic NPs to the Au electrode surface modified with Au NPs (ca. 1.4 nm) yields a microenvironment with a low dielectric constant that results in the single-electron quantum charging of the Au NPs.
In this paper, methods of sample preparation for potentiometric measurement of phenylalanine are presented. Basing on the spectrophotometric measurements of phenylalanine, the concentrations of reagents of the enzymatic reaction (10 mM L-Phe, 0,4 mM NAD+, 2U L-PheDH) were determined. Then, the absorption spectrum of the reaction product, NADH, was monitored (maximum peak at 340 nm). The results obtained by the spectrophotometric method were compared with the results obtained by the colourimetry, using pH indicators. The above-mentioned two methods will be used as references for potentiometric measurements of phenylalanine concentration.
Novel organic membrane-based thin-film microsensors for the determination of heavy metal cations
(2006)
A first step towards the fabrication and electrochemical evaluation of thin-film microsensors based on organic PVC membranes for the determination of Hg(II), Cd(II), Pb(II) and Cu(II) ions in solutions has been realised. The membrane-coating mixture used in the preparation of this new type of microsensors is incorporating PVC as supporting matrix, o-nitrophenyloctylether (o-NPOE) as solvent mediator and a recently synthesized Hg[dimethylglyoxime(phene)]2+ and Bis-(4-hydroxyacetophenone)-ethylenediamine as electroactive materials for Hg(II) and Cd(II), respectively. A set of three commercialised ionophores for Cd(II), Pb(II) and Cu(II) has been also used for comparison. Thin-film microsensors based on these membranes showed a Nernstian response of slope (26-30 mV/dec.) for the respective tested cations. The potentiometric response characteristics (linear range, pH range, detection limit and response time) are comparable with those obtained by conventional membranes as well as coated wire electrodes prepared from the same membrane. The realisation of the new organic membrane-based thin-film microsensors overcomes the problem of an insufficient selectivity of solid-state-based thinfilm sensors.
The applicability of differential pulse voltammetry (DPV) and adsorptive stripping voltammetry (AdSV) at a non-toxic meniscus-modified silver solid amalgam electrode (m-AgSAE) for the determination of trace amounts of genotoxic substances was demonstrated on the determination of micromolar and submicromolar concentrations of 3-nitrofluoranthene using methanol - 0.01 mol L-1 NaOH (9:1) mixture as a base electrolyte and of Ostazine Orange using 0.01 mol L-1 NaOH as a base electrolyte.
This paper presents a two-dimensional-in-space mathematical model of biosensors based on an array of enzyme microreactors immobilised on a single electrode. The modeling system acts under amperometric conditions. The microreactors were modeled by particles and by strips. The model is based on the diffusion equations containing a nonlinear term related to the Michaelis-Menten kinetics of the enzymatic reaction. The model involves three regions: an array of enzyme microreactors where enzyme reaction as well as mass transport by diffusion takes place, a diffusion limiting region where only the diffusion takes place, and a convective region, where the analyte concentration is maintained constant. Using computer simulation, the influence of the geometry of the microreactors and of the diffusion region on the biosensor response was investigated. The digital simulation was carried out using the finite difference technique.
O Perfil Reiss apresenta no resultado uma visão da estrutura dos motivos e impulsos de uma pessoa. O ponto de saída para a análise do resultado é o conhecimento de que os motivos vitais (= valores e metas de sobrevivência) formam a moldura, na qual as competências e capacidades que uma pessoa possui possam se desabrochar de forma ideal. A partir desse princípio, não existe no Perfil Reiss nenhum resultado que se possa classificar como correto ou falso, nem como bom ou mau. Uma comparação entre o resultado do Perfil Reiss e o conteúdo de uma atividade apresentada ou ambicionada dá informação sobre até que ponto a capacidade de rendimento de uma pessoa nessa posição pode vir ou virá a se desenvolver por um longo tempo.
Para Reiss, a avaliação de cada um dos 16 motivos vitais é a chave para não só entender o comportamento humano, como também para poder prevê-lo. Tal previsão é também a meta de cada ciência. Quando se quer saber a reação das pessoas, precisa-se primeiro descobrir, o que as pessoas realmente querem – e, então prever, que elas satisfarão esses desejos e necessidades em suas ações. As chances, que o Perfil Reiss oferece, resultam entre outras também, que aqui é possível pela primeira vez uma individualização total. Cerca de 6 bilhões de perfis individuais podem ser apresentados com o Perfil Reiss. Na combinação correta da formação e utilização da tipologia de um lado e da individualidade da conclusão de outro lado, está a força positiva desse instrumento.
This paper reports a first microbial biosensor for rapid and cost-effective determination of organophosphorus pesticides fenitrothion and EPN. The biosensor consisted of recombinant PNP-degrading/oxidizing bacteria Pseudomonas putida JS444 anchoring and displaying organophosphorus hydrolase (OPH) on its cell surface as biological sensing element and a dissolved oxygen electrode as the transducer. Surfaceexpressed OPH catalyzed the hydrolysis of fenitrothion and EPN to release 3-methyl-4-nitrophenol and p-nitrophenol, respectively, which were oxidized by the enzymatic machinery of Pseudomonas putida JS444 to carbon dioxide while consuming oxygen, which was measured and correlated to the concentration of organophosphates. Under the optimum operating conditions, the biosensor was able to measure as low as 277 ppb of fenitrothion and 1.6 ppm of EPN without interference from phenolic compounds and other commonly used pesticides such as carbamate pesticides, triazine herbicides and organophosphate pesticides without nitrophenyl substituent. The applicability of the biosensor to lake water was also demonstrated.
E-Learning AutoCAD
(2006)
Schrittweise Einführung in die Welt des AutoCAD. Nach jedem Abschnitt besteht die Möglichkeit, das neue Wissen direkt anzuwenden. Mit Wissensprüfungen und Übungen nach jedem Kapitel. (Modul wird noch überarbeitet) 1. Der Anfang mit AutoCAD 2. Grundlagen zur Anfertigung einer Zeichnung 3. Layer 4. Texte und Bemaßung 5. Weiterführende Zeichenwerkzeuge 6. Layout und Plotten
E-Learning Access
(2006)
Schrittweise Einführung in Access. Nach jedem Abschnitt besteht die Möglichkeit, das neue Wissen direkt anzuwenden. Mit Wissensprüfungen und Übungen nach jedem Kapitel. 1. Grundbegriffe aus der Datenbank 2. Eine Datenbank planen 3. Tabellen erstellen und bearbeiten 4. Abfragen erstellen und bearbeiten 5. Formulare - Tuning für die Daten 6. Berichte - echt einfach
In: Technical feasibility and reliability of passive safety systems for nuclear power plants. Proceedings of an Advisory Group Meeting held in Jülich, 21-24 November 1994. - Vienna , 1996. - Seite: 43 - 55 IAEA-TECDOC-920 Abstract: It is shown that the difficulty for probabilistic fracture mechanics (PFM) is the general problem of the high reliability of a small population. There is no way around the problem as yet. Therefore what PFM can contribute to the reliability of steel pressure boundaries is demonstrated with the example of a typical reactor pressure vessel and critically discussed. Although no method is distinguishable that could give exact failure probabilities, PFM has several additional chances. Upper limits for failure probability may be obtained together with trends for design and operating conditions. Further, PFM can identify the most sensitive parameters, improved control of which would increase reliability. Thus PFM should play a vital role in the analysis of steel pressure boundaries despite all shortcomings.
"Mit dem "1. Erfahrungsaustausch" im Fachbereich Bauingenieurwesen berichten Absolventen des Fachbereichs aus der Praxis. Mit diesem Treffen wird die wichtige Verbindung zwischen Hochschule, ihren Absolventen und der Berufspraxis zum besonderen Anliegen gemacht und besonders gestärkt." Zitat Prof. Dr.- Ing. Hans Boegershausen, Dekan im Grußwort. Referenten und Themen: Wellmann, Judith: Perspektiven eines Bauingenieurs im konstruktiven Ingenieurbau Dirk Gobbele, Dirk: Planung der Umbaumaßnahme Hauptbahnhof Aachen Kretschmann, Lars: Planung und Bauleitung Buschtunnel Aachen Becker, Astrid: Anlagenmanagement und Aufgaben der DB Netz AG, Bauherrenvertretung und Wirtschaftlichkeit Plenz, Michael: Baurevision und Unternehmensberatung, Tätigkeit als öffentlich bestellter und vereidigter Sachverständiger Klöcker, Alexander: Das Leitungsbauunternehmen – Unternehmerische Strategie als Zukunftssicherung Türk, Roman: Sanierung von Hausanschlüssen Bornebusch, Michael: Hydraulische und Hydrologische Modellsimulationen als Planungswerkzeug für Hochwasser-Schutz-Maßnahmen Himmerich, Jörg : Pipeline Integrity Management System – Probabilistische Bewertung von Bauwerken am Beispiel von Hochdruckleitungen.
In: Alfha.net / Sektion Bauingenieurwesen: 1. [Erster] Erfahrungsaustausch : Absolventen des Fachbereichs Bauingenieurwesens berichten. 13. Oktober 2006. S. 16-17 Der Umbau des Aachener Buschtunnels im Rahmen des europäischen Hochgeschwindigkeitsschienennetzes wird im sogenannten "Neuen Österreichischen Tunnelbauverfahren (NOeT)", also ein Ausbau in Kalotte, Strosse und Sohle durchgeführt.
In: Alfha.net / Sektion Bauingenieurwesen: 1. [Erster] Erfahrungsaustausch : Absolventen des Fachbereichs Bauingenieurwesens berichten. 13. Oktober 2006. S. 19-20. Zusammenfassung des Vortrags: Prozessanalyse und Revision beim Umbau des Flughafens Hamburg, Beratung von Bauunternehmen, Sachverständigentätigkeit