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In this study, a recently proposed NMR standardization approach by 2H integral of deuterated solvent for quantitative multicomponent analysis of complex mixtures is presented. As a proof of principle, the existing NMR routine for the analysis of Aloe vera products was modified. Instead of using absolute integrals of targeted compounds and internal standard (nicotinamide) from 1H-NMR spectra, quantification was performed based on the ratio of a particular 1H-NMR compound integral and 2H-NMR signal of deuterated solvent D2O. Validation characteristics (linearity, repeatability, accuracy) were evaluated and the results showed that the method has the same precision as internal standardization in case of multicomponent screening. Moreover, a dehydration process by freeze drying is not necessary for the new routine. Now, our NMR profiling of A. vera products needs only limited sample preparation and data processing. The new standardization methodology provides an appealing alternative for multicomponent NMR screening. In general, this novel approach, using standardization by 2H integral, benefits from reduced sample preparation steps and uncertainties, and is recommended in different application areas (purity determination, forensics, pharmaceutical analysis, etc.).
Der digitale Transformationsprozess ist einer der größten gesellschaftlichen Umbrüche in der Geschichte der Menschheit. Aufgrund der Corona-Pandemie stieg die Nutzung von digitalen Kanälen bei den Bürger:innen wie nie zuvor und führt zu einem sprunghaften Anstieg der Nachfrage nach öffentlichen Services in digitaler Form.
Das Ziel dieser Bachelorarbeit ist es, einen digitalen Raum zu gestalten, der den analogen Weg zum Amt größtenteils erspart. Mit geeigneten Kommunikationskanälen kann auf die Bedürfnisse unterschiedlicher Gruppen eingegangen werden. Die Entwicklung der Anwendung IDport bietet sowohl private als auch staatliche Einsparpotenziale. Bürokratische Aufwände sollen durch eine neue Art des E-Government beseitigt werden. Die Konzeption ist infolge der aktuellen Gegebenheit in Deutschland weit entfernt von einer realitätsnahen Umsetzung, weshalb es sich bei der Anwendung um eine revolutionäre Zukunftsvision handelt.
Past earthquakes demonstrated the high vulnerability of industrial facilities equipped with complex process technologies leading to serious damage of the process equipment and multiple and simultaneous release of hazardous substances in industrial facilities. Nevertheless, the design of industrial plants is inadequately described in recent codes and guidelines, as they do not consider the dynamic interaction between the structure and the installations and thus the effect of seismic response of the installations on the response of the structure and vice versa. The current code-based approach for the seismic design of industrial facilities is considered not enough for ensure proper safety conditions against exceptional event entailing loss of content and related consequences. Accordingly, SPIF project (Seismic Performance of Multi- Component Systems in Special Risk Industrial Facilities) was proposed within the framework of the European H2020 - SERA funding scheme (Seismology and Earthquake Engineering Research Infrastructure Alliance for Europe). The objective of the SPIF project is the investigation of the seismic behavior of a representative industrial structure equipped with complex process technology by means of shaking table tests. The test structure is a three-story moment resisting steel frame with vertical and horizontal vessels and cabinets, arranged on the three levels and connected by pipes. The dynamic behavior of the test structure and installations is investigated with and without base isolation. Furthermore, both firmly anchored and isolated components are taken into account to compare their dynamic behavior and interactions with each other. Artificial and synthetic ground motions are applied to study the seismic response at different PGA levels. After each test, dynamic identification measurements are carried out to characterize the system condition. The contribution presents the numerical simulations to calibrate the tests on the prototype, the experimental setup of the investigated structure and installations, selected measurement data and finally describes preliminary experimental results.
Past earthquakes demonstrated the high vulnerability of industrial facilities equipped with complex process technologies leading to serious damage of process equipment and multiple and simultaneous release of hazardous substances. Nonetheless, current standards for seismic design of industrial facilities are considered inadequate to guarantee proper safety conditions against exceptional events entailing loss of containment and related consequences. On these premises, the SPIF project -Seismic Performance of Multi-Component Systems in Special Risk Industrial Facilities- was proposed within the framework of the European H2020 SERA funding scheme. In detail, the objective of the SPIF project is the investigation of the seismic behaviour of a representative industrial multi-storey frame structure equipped with complex process components by means of shaking table tests. Along this main vein and in a performance-based design perspective, the issues investigated in depth are the interaction between a primary moment resisting frame (MRF) steel structure and secondary process components that influence the performance of the whole system; and a proper check of floor spectra predictions. The evaluation of experimental data clearly shows a favourable performance of the MRF structure, some weaknesses of local details due to the interaction between floor crossbeams and process components and, finally, the overconservatism of current design standards w.r.t. floor spectra predictions.
Ängste und Phobien sind vielseitig. Furcht im Alltag spiegelt sich sowohl in spezifischen Objekten als auch in allgemeinen Situationen wider. Für unbetroffene Menschen sind diese Emotionen oft unbegreiflich, irrational und abstrakt.
In 15 Bildergeschichten werden verschiedene persönliche Ängste humoristisch illustriert und in einer gebundenen Comic-Anthologie zusammengeführt. Der überzogene, bizarre Zeichenstil demonstriert die empfundene Wahrnehmung bei alltäglichen Ängsten auf eine nicht allzu ernst gemeinte Weise. Zeichnerische Ästhetik, von klassischem Comic-Stil bis zum grafischen Horror, und Storytelling stehen hier im Vordergrund. Lesende finden sich selbst in den absurden Geschichten wieder und werden im besten Fall zum Lachen gebracht.
Die Bachelorarbeit SCHRECKLICHES versucht das abstrakte Gefühl der Angst auf nachvollziehbare Art zeichnerisch und mit einer guten Portion Übertreibung zu vermitteln.
Robotic process automation (RPA) has attracted increasing attention in research and practice. This chapter positions, structures, and frames the topic as an introduction to this book. RPA is understood as a broad concept that comprises a variety of concrete solutions. From a management perspective RPA offers an innovative approach for realizing automation potentials, whereas from a technical perspective the implementation based on software products and the impact of artificial intelligence (AI) and machine learning (ML) are relevant. RPA is industry-independent and can be used, for example, in finance, telecommunications, and the public sector. With respect to RPA this chapter discusses definitions, related approaches, a structuring framework, a research framework, and an inside as well as outside architectural view. Furthermore, it provides an overview of the book combined with short summaries of each chapter.